Chromatography

Shimadzu Analytical & Measuring

Shimadzu’s LabSolutions Unified Laboratory Management System (ULMS) provides a single, easy-to-use interface for multiple types of techniques, including HPLC, LC-MS, GC, ICP-MS, FTIR, and UV-Vis.  It provides extremely efficient laboratory workflows while still providing the high-level functionality and data management required in today's modern laboratory. The unified platform simplifies training, facilitates better data management, and reduces costs.

How a Unified Laboratory Management System Streamlines Your Analysis

Low cost lab automation

Three autosamplers that I built myself and use routinely in the lab. At left and right, microsyringe autosamplers. In the center, an autosampler for elemental analysis. I am not using the last one in this video.
1) EA autosampler ( bit.ly/3erjacu ); 2) Microsyringe autosampler ( bit.ly/2QVnDJU ); 3) Gamma-ray autosampler ( bit.ly/2xxjlQN ); 4) Robotic arm autosampler ( bit.ly/2DCIcs1 ); 5) Portable autosampler for shallow waters (bit.ly/34cHKut)

Three DIY autosamplers

PEAK Scientific

Peak Scientific's Precision SL is the smallest hydrogen generator for GC-FID. The Precision SL line has been designed to offer a streamlined laboratory-grade hydrogen gas solution for GC flame detectors at a purity of 99.9995%, available in both 100 and 200cc/min. Precision is safe, simple to use, easy to maintain and takes up minimal bench space.

Precision SL Hydrogen Generator

Be Extraordinary

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SCIEX presents Extraordinary Grace

Analytical Technologies Limited

The instruments fully absorbs advanced technology abroad of the same kind of products, adopts
domestic industrial leading manufacturing technology and process, and ensures instrument
reliability and non-failure operation time. It maximizes normal operation, reduces maintenance,
and makes structure simple, proper, and easy to learn and operate.
It has unique remote network transmission and control function and achieved duty-free,
decentralized monitoring and centralized control; the data analysis results are input into DCS to
nish statistics, analysis,monitoring of the chromatograph group and improve automation of
production process.
It is extensively used in petroleum and chemical industry, ne chemical engineering, biological
pharmaceutical industry, environmental protection, food health, high purity gas, electricity, wine
brewing,scientic research, education and other analyzing elds.

Gas chromatography Demostration by Analytical Technologies Limited

Chromatography & Mass Spectrometry Solutions

Thermo Scientific Chromeleon CDS is built for compliance from the ground up. Learn how Chromeleon software makes it easier to comply with regulations and ensure data integrity in your laboratory.

Chromeleon 7 CDS Software - Built for Compliance

SiliCycle Inc.

E-PAK is a family of radial flow purification cartridges developed specifically for pharmaceutical processing.

Offered with a choice of metal scavengers, bare silica & activated carbons, these cartridges are designed to remove precious metal catalysts, reaction-by-products or color from synthetic reaction mixtures and natural products.

For more information on E-PAK, visit us at:
https://www.silicycle.com/products/e-pak-purification-cartridges

How to select right sized E-PAK cartridges?

Radleys

In this video we demonstrate how to correctly align the overhead stirrer on the Reactor-Ready jacketed lab reaction system. 

Correct alignment of your overhead stirrer will ensure there is no whip of the impeller, reducing the risk of wear on the stirrer guide bearing as well as PTFE shedding of the impeller into the vessel.

Radleys' Reactor-Ready jacketed laboratory reactor system, is designed as a universal jacketed lab reactor work station with a range of easily interchangeable vessels from 100 ml to 5 litres which can be configured to suit the chemistry and scale needed for each project. 

Easy to use, this one unique framework can replace many jacketed lab reactors, saving money and fumehood space by using one circulator with multiple setups. Reactor-Ready is ideal for organic chemistry, process chemistry, process development, medicinal chemistry, R&D research, polymer chemistry, academic research, API manufacture and CRO or contract synthesis. 

Reactor-Ready features: 

• Rapid vessel exchange with quick-release vessel clamps and wide bore hose couplings. 
• Range of standard (single and vacuum jacketed) glass reactor vessel – 250 ml to 5 L. 
• Range of process (single and vacuum jacketed) glass reactor vessel - 100 ml to 5 L Process Vessels. 
•Mimic the geometry of plant scale reactors and feature a 1.25 to 1 ratio of internal height to internal diameter, with dish shaped bottom. 
• DN100 vessel flange. 
• Accepts all leading brands of overhead stirring and allows easy, tool free adjustment. 
• Compact stainless-steel framework accepts all vessel sizes. 
• Self aligning stirrer coupling engages without the need for tools. 
• Temperature range: -70 ˚C to +230 ˚C (thermofluid temperature).
• Innovative hose manifolds allow easy thermofluid drain down. 
• Wide range of accessory glassware including condensers, dropping funnels etc. 
• Optional software allows you to log and control 3rd party devices. 

Reactor-Ready also offers a range of accessories such as condensers, temperature probes, glass and PTFE lids, PTFE impellers and reflux divider kits. You can also automate your jacketed lab reactor system with our AVA Lab Control Software which controls and data logs all the periphery devices connected to your jacketed lab reactor, such as overhead stirrers, circulators and gravimetric additions modules for accurate liquid dosing. 

For more information visit: https://www.radleys.com/range/reactor-ready-lab-reactor
Book a demo and learn more about Reactor Ready here: https://www.radleys.com/range/reactor-ready-lab-reactor/

Instagram: https://www.instagram.com/radleys_chemistry
Facebook: https://www.facebook.com/radleyschemistry
LinkedIn: https://www.linkedin.com/company/77309​
Twitter: https://twitter.com/Radleys​

#jacketedlabreactor #processchemistry #jacketed reactor

How to easily align an overhead stirrer on a Radleys jacketed glass reactor

In this video, Dr Nilesh Mistry gives you an introduction to the Radleys parallel synthesis range and an insight into how they may help your small molecule synthesis projects. 

Working on small molecule discovery, reaction optimisation or reagent screening? 
Need to increase your experimental throughput without compromising on your set-up? 
Want to perform multiple reactions in parallel, but have limited fume hood space? 

Chemists and engineers at GlaxoSmithKline were instrumental in developing a range of clever parallel synthesis tools designed to tackle performing multiple reactions on one magnetic stirrer hot plate. 

Developed in a partnership between GSK chemists and Radleys engineers: The Radleys Carousel 12, Radleys Carousel 6 and the Radleys GreenHouse parallel synthesiser and blowdown unit are easy to use, perform multiple reactions, fit on a standard magnetic stirrer hot plate and take up less space than multiple individual set-ups. 

Parallel synthesis tools are a great addition to your chemistry lab equipment and ideal for the following organic and inorganic chemistry applications: medicinal chemistry, reaction screening, combinatorial chemistry, catalyst screening, drug discovery, parallel solution phase chemistry, solid supported reagent based synthesis and much more. 

Heat, cool, stir and reflux multiple reactions under an inert atmosphere on a single magnetic stirrer hot plate. 

Carousel 12 Plus Reaction Station: 
The patented Carousel 12 Plus simultaneously heats/cools, stirs and refluxes multiple reactions under an inert atmosphere. An effective personal synthesis station for parallel chemistry and solid supported reagent screening synthesis. 
• Accepts up to 12 glass tubes with a reaction volume from 1 ml to 20 ml 
• Powerful, even stirring – fits on to a Carousel stirring hotplate 
• Rapid heating to 220 ˚C and cooling to -78 ˚C 
• Quick to set-up and easy to use 
• Easy viewing of tube contents during experiments 
• Removable water-cooled refluxing head 

GreenHouse Plus Parallel Synthesiser: 
The GreenHouse Plus provides 24 heated and stirred glass reactions with volumes from 0.5 ml to 7 ml. The refluxing head allows for convenient additions or withdrawals whilst maintaining an inert atmosphere. 
• Powerful stirring and rapid heating to 150 ˚C 
• 24 tube, micro titer plate footprint 
• Reaction volumes from 0.5 ml to 7 ml 
• Removable water-cooled reflux head 
• Perform reactions under an inert atmosphere 
• Easy viewing of tube contents during experiments 
• Nickel plated aluminium offers excellent chemical resistance 

Carousel 6 Plus Reaction Station: 
The patented Carousel 6 Plus offers parallel chemistry in the most universally accepted chemistry reaction vessel, the round bottom flask. 
• Accepts round bottom flasks, including vessels with one or two sidearms: 5 ml, 10 ml, 25 ml, 50 ml, 100 ml, 170 ml and 250 ml. 
• Powerful, even stirring – fits on to a Carousel stirring hotplate 
• Rapid heating to 180 ˚C and cooling to -78 ˚C 
• Quick to set-up and easy to use 
• Water-cooled reflux head 

For more information on this range visit https://www.radleys.com/range/parallel-reaction-stations 
To book a demo with an expert visit: https://calendly.com/parallel-reaction-stations 

Instagram: https://www.instagram.com/radleys_chemistry 
Facebook: https://www.facebook.com/radleyschemistry 
LinkedIn: https://www.linkedin.com/company/77309 
Twitter: https://twitter.com/Radleys 

#chemistry #realtimechem #parallelsynthesis

Chromatography

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